@Article{MarcuzzoCuTaMeBeBa:2016:PrChAp,
author = "Marcuzzo, Jossano Saldanha and Cuña, Andres and Tancredi, Nestor
and Mendez, Eduardo and Bernardi, Heide Heloise and Baldan,
Maur{\'{\i}}cio Ribeiro",
affiliation = "{Instituto Nacional de Pesquisas Espaciais (INPE)} and
{Universidad del Uruguay} and {Universidad del Uruguay} and
{Universidad de la Rep{\'u}blica} and {Faculdade de Tecnologia do
Estado de S{\~a}o Paulo} and {Instituto Nacional de Pesquisas
Espaciais (INPE)}",
title = "Microporus activated carbon fiber felt from Brazilian textile PAN
fiber: preparation, characterization and application as super
capacitor electrode",
journal = "Revista Brasileira de Aplica{\c{c}}{\~o}es de V{\'a}cuo",
year = "2016",
volume = "35",
number = "2",
pages = "58--63",
month = "Maio-Ago.",
keywords = "Activated carbon fiber, Activated felt, Supercapacitor electrodes,
Fibra de carbono ativada, Feltro ativado, Eletrodo
supercapacitor.",
abstract = "Activated carbon fibers (ACF) are known as excellent adsorbent
materials due to their fast adsorption rate and easy handling
characteristic. The ACF can be manufactured from the
polyacrylonitrile fiber, based on an usual carbon fibers (CF)
production process accomplished by an additional activation
process. The aim of the present work is to describe the
production, chemical/morphological characterization and
application potentiality of activated carbon fiber felt (ACFF)
produced from textile PAN fiber, using a set of homemade
equipment. The 5.0 dtex PAN fiber tow with 200 thousand filaments
was oxidized and used as raw material for felt production. The
oxidized PAN fiber felt (OPFF) was displaced in a special sample
holder, carbonized (900 °C) and then activated in CO2 atmosphere
at 1000 °C in an electric tubular furnace. All steps of the
process were performed as fast as possible, and characterization
was done by 77 K N2 isotherms, adsorption isotherms in liquid
phase, scanning electronic microscope, X-ray diffraction and
surface chemistry by Bhoem methodology. The results confirmed the
production of essentially microporous (pore < 3.2 nm, centered on
1.2 nm) and 1,300 m2 g-1 surface area. The ACFF produced have
demonstrated a strong potential application as electrode
supercapacitor. RESUMO: Fibras de carbono ativado (FCA) s{\~a}o
conhecidas por ser um excelente material adsorvente devido sua
elevada cin{\'e}tica de adsor{\c{c}}{\~a}o e facilidade de
manuseio. As FCA podem ser produzidas a partir da fibra de
poliacriolonitrila e mesmo processo utilizado na
fabrica{\c{c}}{\~a}o de fibras de carbono, acoplando-se uma
etapa de ativa{\c{c}}{\~a}o ao final do processo. Neste trabalho
{\'e} descrito a produ{\c{c}}{\~a}o, caracteriza{\c{c}}{\~a}o
qu{\'{\i}}mica/morfol{\'o}gica e potencial
aplica{\c{c}}{\~a}o de feltros de fibra de carbono ativado
(FFCA), produzidos a partir de fibra PAN t{\^e}xtil nacional em
um equipamento experimental. Fibras PAN de 5.0 dtex em cabo de 200
mil filamentos foram oxidadas termicamente e utilizadas como
mat{\'e}ria prima para a produ{\c{c}}{\~a}o de feltro. O feltro
de fibra PAN oxidada (FFPO) foi colocada em um porta amostra,
especialmente desenhado, e inserido em um forno tubular
el{\'e}trico, carbonizado (900 °C) e em seguida ativado em
atmosfera de CO2 a 1000 °C. Todas as etapas foram feitas na maior
taxa poss{\'{\i}}vel e as caracteriza{\c{c}}{\~o}es foram
feitas por isotermas de N2 a 77 K, a qu{\'{\i}}mica de
superf{\'{\i}}cie foi analisada por titula{\c{c}}{\~a}o de
Bhoem. Os resultados mostram um material essencialmente
microporoso (poros < 3,2nm, concentrados em 1,2 nm) e 1300 m2 de
{\'a}rea espec{\'{\i}}fica. O material produzido apresentou
forte indicativo de aplica{\c{c}}{\~a}o como eletrodo de
supercapacitor.",
doi = "10.17563/rbav.v35i2.1022",
url = "http://dx.doi.org/10.17563/rbav.v35i2.1022",
issn = "0101-7659",
language = "en",
targetfile = "marcuzzo_microporus.pdf",
urlaccessdate = "27 abr. 2024"
}